Microwave-assisted synthesis of nanorod hydroxyapatite from eggshells

oleh: Doan Van Hong Thien, Nguyen Thi Bich Thuyen, Tran Thi Bich Quyen, Nguyen Huu Chiem, Van Pham Dan Thuy, Pham Hung Viet

Format: Article
Diterbitkan: Vietnam Ministry of Science and Technology 2021-03-01

Deskripsi

Nanorod hydroxyapatite (HA) was synthesised from eggshells by using a microwave-assisted technique. With eggshells and phosphoric acid as precursors, the reaction was carried out in a microwave with an irradiation power of 800 W for 45 minutes. The effects of Ca/P molar ratios and the power of microwaves were investigated. The obtained hydroxyapatite was characterised by X-ray diffraction (XRD), scanning electron microscope (SEM), and infrared spectroscopy (IR). The nanorod-like HA samples were 20-40 nm in diameter and 130-180 nm in length.