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In the light of the alarming impending energy scene, energy efficiency and exergy efficiency are unmistakably gathering momentum. Among efficient process design methodologies, literature suggests pinch analysis and exergy analysis as two powerful thermodynamic methods, each showing certain drawbacks, however. In this perspective, this article puts forward a methodology that couples pinch and exergy analysis in a way to surpass their individual limitations in the aim of generating optimal operating conditions and topology for industrial processes. Using new optimizing exergy-based criteria, exergy analysis is used not only to assess the exergy but also to guide the potential improvements in industrial processes structure and operating conditions. And while pinch analysis considers only heat integration to satisfy existent needs, the proposed methodology allows including other forms of recoverable exergy and explores new synergy pathways through conversion systems. A simple case study is proposed to demonstrate the applicability and efficiency of the proposed method.