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<b>Determination of cypermethrin residues in <i>Gingkgo biloba<i> leaves by high performance liquid chromatography</b>
oleh: Jin-Jun Zhang, Li-Guo Zang, Jin-E Zhang, Guan-Wei Cui, Bo Tang, Xiang-Yang Li, Li Zhou
Format: | Article |
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Diterbitkan: | Chemical Society of Ethiopia 2009-04-01 |
Deskripsi
A simple and rapid method was described for the determination of cypermethrin in <i>Ginkgo biloba</i> leaves by high performance liquid chromatography (HPLC) with UV detection. A mixture of hexane and acetone (99:1) was used to extract the samples. After the sample cleanup was carried out with a mixture of petroleum ether and ethyl acetate (9:1) cypermethrin in the sample was analyzed using a Phenomenex Luna 5 micron second-generation silica column packed with Florisil and active carbon. The recovery of cypermethrin was 81.0% and the relative standard deviation was 3.2%.