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A Versatile Broadband Attached Proton Test Experiment for Routine <sup>13</sup>C Nuclear Magnetic Resonance Spectroscopy
oleh: Peter Bigler, Ilche Gjuroski, Dib Chakif, Julien Furrer
| Format: | Article |
|---|---|
| Diterbitkan: | MDPI AG 2024-02-01 |
Deskripsi
The proposed broadband attached proton test sequence allows the user to easily record <sup>13</sup>C nuclear magnetic resonance multiplicity-edited and quaternary-carbon-only spectra. Compared to earlier attached proton test experiments, it preserves both a tolerance for wide ranges of one-bond-coupling constant values and the effective suppression of residual CHn signals in the quaternary-carbon-only spectra. The recording of edited spectra or quaternary-carbon-only spectra is made easy by a single, user-controllable constant. These attributes make the broadband attached proton test experiment attractive for the <sup>13</sup>C analysis of small molecules, including spectral editing, particularly in high-throughput analysis laboratories.