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In this study, TiO₂ nanofibers were prepared with Polyvinylpyrrolidone (PVP) polymer using sol-gel method via electrospinning technique. Owing to the advantages of small fiber diameter, tunable porosity, low cost, large surface to volume ratio, structure control, light-weight, and less energy consumption, electrospun nanofibers are evolving as an adaptable material with a number of applications, in this case for filtration and environmental/virus protection. Different samples of TiO₂/PVP nanofibers have been prepared by changing the parameters to achieve the best result. As the polymer concentration was increased from 6 to 8 wt.% of PVP, diameter of the resultant fibers was seen to be increased, implying decrease in the pore-size of the fibers up to 1.4 nm. Surface morphology has been checked via Scanning Electron Microscope (SEM) images. Crystalline nature has been analyzed by X-ray Crystallography. Using the Bruanauer-Emmett-Teller (BET) test, surface area and porosity has been checked for the suitable application. The synthesized TiO₂/PVP nanofibers have tremendous practical potentials in filtration and environmental remediation applications.