Pinacol Coupling of Aromatic Aldehydes using La-Ticl4 in CH3COOEt under Ultrasound Irradiation
oleh: Ji-Tai Li, Xue-Li Sun, Zhi-Ping Lin, Tong-Shuang Li
| Format: | Article |
|---|---|
| Diterbitkan: | Wiley 2006-01-01 |
Deskripsi
Titanium tetrachloride can be reduced by lanthanum filings to the corresponding low valent titanium complex, which can induce some aromatic aldehydes to the corresponding pinacols in 28%-97% yields within 10-50 min in ethyl acetate at r.t. under ultrasound irradiation.