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Microstructure Evolution and Effect on Deuterium Retention in TiC- and ZrC-Doped Tungsten under He<sup>+</sup> Ion Irradiation
oleh: Xiaoyu Ding, Jiahui Fang, Qiu Xu, Panpan Zhang, Haojie Zhang, Laima Luo, Yucheng Wu, Jianhua Yao
Format: | Article |
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Diterbitkan: | MDPI AG 2023-04-01 |
Deskripsi
Combining the advantages of a wet chemical method and spark plasma sintering, carbide-doped materials W-1wt%TiC and W-1wt%ZrC were prepared. Microstructural evolution in W-1wt%TiC and W-1wt%ZrC under irradiation of 5 keV He<sup>+</sup> at 600 °C to fluences up to 5.0 × 10<sup>21</sup> ions/m<sup>2</sup> with ion flux of about 8.8 × 10<sup>17</sup> ions/m<sup>2</sup>s was investigated by transmission electron microscopy (TEM). The dislocation loop number density of W-1wt%TiC was higher than that of W-1wt%ZrC, but the average loop size of the W-1wt%TiC was in average smaller. There were no observable helium bubbles in W-1wt%TiC and W-1wt%ZrC, exhibiting higher radiation resistance to He<sup>+</sup> compared to pure W. He<sup>+</sup> pre-damaged and undamaged W-1wt%TiC and W-1wt%ZrC samples were irradiated by 5 keV D<sub>2</sub><sup>+</sup> to estimate the D retention in doped W materials. The irradiation damage impact of He<sup>+</sup> on deuterium retention was examined by a method of thermal desorption spectroscopy (TDS). Compared with the undamaged samples, it was illustrated that D<sub>2</sub> retention of W-1wt%TiC and W-1wt%ZrC increased after He<sup>+</sup> pre-irradiation.