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Stability of Nanocrystalline Spark Plasma Sintered 3Y-TZP
oleh: Marc Anglada, Michael Reece, Haixue Yan, Fernando García Marro, Alvaro Mestra, Ravikiran Chintapalli
Format: | Article |
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Diterbitkan: | MDPI AG 2010-01-01 |
Deskripsi
Spark plasma sintered 3Y-TZP has been investigated with respect to hydrothermal ageing and grinding. The sintering was performed between the temperatures of 1,100 and 1,600 °C for a soaking time of 5 minutes and the resulting materials were obtained with grain sizes between 65 to 800 nm and relative densities between 88.5 to 98.8%. Experiments on hydrothermal ageing in water vapour at 131 °C, 2 bars during 60 hours shows that phase stability is retained, elastic modulus and hardness of near surface region measured by nanoindentation does not change in fine grain (<200 nm) materials, in spite of porosity. In ground specimens, very small amount of transformation was found for all grain sizes studied.