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The utilization of natural fibre-based biodegradable polymers has expanded in the present circumstances since natural fibres are relatively inexpensive, recyclable, lighter, nonflammable, and harmless. However, hydrophilic nature is the most serious issue. To address this issue, the current study was applied to enhance the material characteristics of hybrid composites strengthened by CGF and nanosilica powder. To accomplish the mentioned goal, RSM calculated and optimized the following processing parameters using the BBD arrangement at various CGF fibre thickness (gsm), weight percent of nanosilica powder (wt. percent), and cryogenic treatment period (min). To prevent hydrophilic nature, the fibres were pretreated for four hours with a 5% alkaline solution. Deterioration models were created to analyze the material characteristics, and the optimal progression variables were determined. Based on the multiresponse surface methodology, the governable process variables for nano-silica- and CGF-based hybrid nanocomposites should be set at 3% silica, 300 gsm of CGF, and 30 minutes of cryogenic treatment. The tension, bending, and impact property correlation coefficient values (R2) are 0.95, 0.94, and 0.95, respectively. The above-mentioned combinations provide better water absorption and mechanical strength.