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A simple scheme for single-channel coherent perfect absorption (CPA) of transparent materials is proposed and experimentally realized using total internal reflection by grazing incidence, with a single dielectric layer sandwiched by semi-infinite dielectric layers. In a 1.48-µm thick polyvinylpyrrolidone (PVP) film, dip-coated on a MgF₂ substrate both transparent in the visible, reflectance dips due to nearly 90% absorption by single-channel CPA were observed in the wavelength range of 370–800 nm, with white light from a Xe lamp incident on the side face of the substrate and extracted from the other side through multiple reflections in the PVP layer. This is a simple and inexpensive CPA scheme, and it is expected to have various applications by changing the substrate/polymer material or dispersing molecules in the polymer film. This paper also provides a design guideline for grazing-incidence waveguide-mode sensors using transparent dielectric materials.