RAPID SOLVENT-FREE MICROWAVE ASSISTED SYNTHESIS OF SOME N’-BENZYLIDENE SALICYLIC ACID HYDRAZIDES

oleh: Tutuk Budiati, Stephanie D.A., Elisabeth Catherina Widjajakusuma

Format: Article
Diterbitkan: Department of Chemistry, Universitas Gadjah Mada 2012-06-01

Deskripsi

Condensation reaction has been carried out for the synthesis of some N'-benzylidene-2-hydroxybenzohydrazides using microwave assisted solvent-free method. The structures of all the products obtained in the present work are supported by spectral and analytical data (UV, IR, and 1H-NMR spectroscopy). The desired hydrazides are in 62-80% yields under microwave irradiation. The reaction was completed in 8-10 min.