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Metal oxide nanoparticles have captivated scrupulous research interest because of its major relevance in the field of medicine, catalysis, pigment, electronics, biotechnology, sensors, optical devices, adsorption, DNA labelling, drug delivery, kinetics, spintronics and piezoelectricity. Nanoparticles (NPs) became more significant for its reasonable property as a heterogeneous non-toxic catalyst with environmental reimbursement. The biogenic innovation of metal oxide NPs is an enhanced alternative owing to eco-friendliness. In the biological field, the probable efficacy of NPs has been reported by scores of scholars in the treatment of cancer. Owed to munificent returns, NPs explored as a powerful catalyst for several organic transformations. This section unlocks with a short course on to synthesize metal oxide NPs on a natural scale.