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Pre-concentration and determination of Zn (II) across a ligand assisted pseudo stirbar hollow fiber solid/liquid phase microextraction method in water samples has been investigated. All detections were carried out by differential pulse anodic stripping voltammetry (DPASV). The method involves microextraction and pre-concentration of Zn (II) on the pseudo stir bar hollow fiber. Then desorption has been done using suitable solvent containing suitable ligand as complexing agent. The optimized conditions were obtained. The relationship between the peak current and concentration was linear over the range of 0.05–500 ng mL−1. The limit of detection was 0.015 ng mL−1. Under the optimized conditions, the pre-concentration factor is 5140. The applicability of the developed technique was evaluated by application to spiked, environmental water samples.