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Continuous Flow Alcoholysis of Dialkyl H-Phosphonates with Aliphatic Alcohols
oleh: Erika Bálint, Ádám Tajti, Nóra Tóth, György Keglevich
Format: | Article |
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Diterbitkan: | MDPI AG 2018-07-01 |
Deskripsi
The continuous flow alcoholysis of dialkyl H-phosphonates by aliphatic alcohols in the absence of a catalyst was elaborated using a microwave (MW) reactor equipped with a flow cell. By the precise control of the reaction conditions, the synthesis could be fine-tuned towards dialkyl H-phosphonates with two different and with two identical alkyl groups. In contrast to the “traditional” batch alcoholysis, flow approaches required shorter reaction times, and the products became available at a larger scale.