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Creep Mechanisms of an Al–Cu–Mg Alloy at the Macro- and Micro-Scale: Effect of the S′/S Precipitate
oleh: Yongqian Xu, Lingwei Yang, Lihua Zhan, Hailiang Yu, Minghui Huang
Format: | Article |
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Diterbitkan: | MDPI AG 2019-09-01 |
Deskripsi
A novel methodology combining the macro- and micro-creep techniques was employed to study the effect of S′/S precipitate growth on the creep mechanism of an Al−Cu−Mg alloy. An AA2524 alloy was pre-aged at 180 °C to obtain S′/S precipitates with various sizes. The results showed that the precipitate size increased approximately linearly to ≈32 nm, ≈60 nm, and ≈105 nm after 3 h, 6 h, and 12 h of pre-aging, respectively. The growth of precipitate could significantly shorten the primary creep stage, despite the fact that the steady-state creep behavior was similar to that of the as-received alloy, as revealed by the macro tensile creep tests at 180 °C and 180 MPa. This led to a stress exponent (2.4−2.5) of the Al alloy with various precipitate sizes that was quite close to that of the as-received Al alloy, implying a steady-state creep mechanism dominated by grain boundary sliding and dislocation interactions. Finally, the micro-creep tests showed a minor role of the precipitate size on the steady-state creep mechanism, as evidenced by the similar strain rate sensitivity (0.0169−0.0186), activation volume (≈27 b<sup>3</sup>), and the results of a detailed transmission electron microscopy analysis of all tested alloys.