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Solvent Resistant O2 Sensor Integrated in Pressured Flow Reactors
oleh: Philipp Sulzer, René Lebl, Torsten Mayr
Format: | Article |
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Diterbitkan: | MDPI AG 2019-01-01 |
Deskripsi
In this contribution we present an optical oxygen sensor that can easily be integrated into continuous flow reactors. The sensors are pressure resistant to up to 8 bars and are able to continuously measure oxygen for several hours in organic solvents. The dynamic range was evaluated up to 42 mmol/L O2 and several calibrations showed the sensors to perform linearly according to Stern-Volmer, which allows convenient two-point calibrations. By using state-of-the-art HPLC connectors and materials the sensor can be implemented at virtually every point of a standard flow reactor. Readout is conducted via a 4-channel USB phase fluorimeter.