Convenient Synthesis of Triphenylphosphine Sulfide from Sulfur and Triphenylphosphine
oleh: Thanh Binh Nguyen
| Format: | Article |
|---|---|
| Diterbitkan: | MDPI AG 2022-03-01 |
Deskripsi
Elemental sulfur (S<sub>8</sub>) was found to react very rapidly (<1 min) with a stoichiometric amount of triphenylphosphine at rt in sufficient amount of solvent (0.2–0.5 mL of solvent/1 mmol of PPh<sub>3</sub>). Compared to the previously described methods, the present procedure constitute excellent access to triphenylphosphine sulfide.