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Nickel composites doped by chromium and calcium fluoride were produced by powder metallurgy. The friction coefficient of the samples containing 20% of the CaF₂ was lower at elevated temperatures (600 °C) than the friction coefficient for the Ni-50%NiCr(80/20) composite (0.14 vs. 0.20). Sample surfaces were analyzed by the scanning electron microscope (SEM). EDS analysis proved tribofilm formation on the surface of the sample with CaF₂ addition. A laser confocal microscope (LCM) was used to investigate the surface condition of the counter-sample after wear tests. The presence of the tribofilm reduced the wear of the frictional pair, and because of that the wear tracks were smooth. Tribofilm limited the abrasive wear and ploughing. Therefore, the tribofilm protected the sample and counter-sample from wear.