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Nanosized Mn₃O₄ nanowires are prepared with KMnO₄ and ethanol in mild conditions by facile hydrothermal method. Hydrothermal reaction temperature is optimized to get uniform nanowires. The prepared Mn₃O₄ nanowires exhibit high activity in the treatment of phenol at acid condition and room temperature. The 20 mg Mn₃O₄ nanowires can efficiently dispose of 50 mL phenol solution (0.2 g·L^−1) at pH 2 and 25 °C. The nanowires before and after phenol treatment are characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD) and X-ray photoelectron spectroscopy (XPS) and the reaction mechanism is discussed.