Hexaethylguanidinium tetrakis(trimethylsilylethynyl)borate diethyl ether monosolvate

oleh: Stefan Oberparleiter, Gerhard Laus, Thomas Gelbrich, Klaus Wurst, Julia Kunze-Liebhäuser, Herwig Schottenberger

Format: Article
Diterbitkan: International Union of Crystallography 2017-05-01

Deskripsi

The solvated molecular salt, C13H30N3+·C20H36BSi4−·C4H10O, was obtained by the reaction of trimethylsilylethyne with boron trichloride in the presence of tert-butyllithium, followed by ion metathesis. The cation exhibits positional disorder and one of the Me3Si groups shows rotational disorder. No significant directional intermolecular interactions are observed.