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Hyperspectral technology is useful for urban studies due to its capability in examining detailed spectral characteristics of urban materials. This study aims to develop a spectral library of urban materials and demonstrate its application in remote sensing analysis of an urban environment. Field measurements were conducted by using ASD FieldSpec 3 Spectroradiometer with wavelength range from 350 to 2500 nm. The spectral reflectance curves of urban materials were interpreted and analyzed. A collection of 22 spectral data was compiled into a spectral library. The spectral library was put to practical use by utilizing the reference spectra for WorldView-2 satellite image classification which demonstrates the usability of such infrastructure to facilitatefurther progress of remote sensing applications in Malaysia.