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Silica, titania, and mixed silica–titania powders have been used as supports for loading 5 wt% Cu, 5 wt% Ag, and 2.5 wt% Cu-2.5 wt% Ag with the aim of providing a series of nanomaterials with antifouling properties. All the solids were easily prepared by the wetness-impregnation method from commercially available chemical precursors. The resulting materials were characterized by several techniques such as X-ray diffraction analysis, X-ray photoelectron spectroscopy, N₂ physisorption, and temperature-programmed reduction measurements. Four selected Cu and Ag SiO₂- and TiO₂-supported powders were tested as fillers for the preparation of marine antifouling coatings and complex viscosity measurements. Titania-based coatings showed better adhesion than silica-based coatings and the commercial topcoat. The addition of fillers enhances the resin viscosity, suggesting better workability of titania-based coatings than silica-based ones. The ecotoxicological performance of the powders was evaluated by Microtox luminescence tests, using the marine luminescent bacterium <i>Vibrio fisheri</i>. Further investigations of the microbiological activity of such materials were carried out focusing on the bacterial growth of <i>Pseudoalteromonas</i> sp., <i>Alteromonas</i> sp., and <i>Pseudomonas</i> sp. through measurements of optical density at 600 nm (OD_600nm).