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The principal features of primary zone determine the performance parameters of the whole combustion chamber, such as the pollutant emissions and combustion efficiency. In this work, flow field and major species concentration measurements are conducted in the primary zone of an aero-engine combustion chamber. The operating conditions such as air inlet temperature, chamber pressure, and air-to-fuel ratio are chosen to replicate the realistic operating conditions. The velocity field and streamlines are obtained by particle imaging velocimetry technology. The concentrations of major species are acquired by a spontaneous Raman scattering system. This article validates the feasibility of two laser diagnostic measurement techniques and presents the initial results under realistic aero-engine conditions.