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The effect of tungsten, aluminum, and cobalt on the mechanical properties of iron-based composites prepared by powder technology was studied. Five samples with different contents of tungsten, aluminum, and cobalt were established. The five samples have the following chemical compositions: (I) full iron sample, (II) 5wt.% tungsten, (III) 5wt.% tungsten-4wt.% cobalt-1wt.% aluminum, (IV) 5wt.% tungsten-2.5wt.% cobalt-2.5wt.% aluminum, and (V) 5wt.% tungsten-1wt.% cobalt-4wt.% aluminum. The mixed composite powders were prepared by mechanical milling, in which 10:1 ball to powder ratio with 350 rpm for 20 h was cold compacted by a diaxial press under 80 bars, then sintered at temperatures ranging from 1050 °C to 1250 °C in an argon furnace. The samples were characterized mechanically and physically using XRD, SEM, a density measuring device, a hardness measuring device, a compression test device, and a tribological device for wear and friction tests. XRD results refer to the formation of different intermetallic compounds such as Fe₇W₆, Al₅Co₂, Fe₂W₂Co and Co₇W₆ with the main peaks of Fe. The good combination of tribological and mechanical properties was recorded for sample number five, which contained 5% W, 4% Al, 1% Co and Fe base, where it obtained the highest wear resistance, largest hardness, acceptable compressive strength, and lowest friction coefficient due to the good combination of hard and anti-friction intermetallic action compared with the other samples. This sample is a good candidate for applications which require high wear resistance and a moderate friction coefficient accompanied with high toughness, like bearing materials for both static and dynamic loading with superior mechanical and tribological properties.