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In this article, the results of preliminary experimental studies related to a fast, non-contact assessment of the AISI 316L stainless austenitic steel surfaces after electrochemical polishing in a magnetic field have been presented. The experiments were realized with the use of a modified angle-resolved scattering (ARS) method based on the analysis of angular distribution of the scattered light intensity. Digital images of such distribution were acquired for selected areas of examined samples—base surface and surface after magnetoelectropolishing (MEP) process. Parametric analysis oriented toward the calculation of selected key geo- and photometric parameters carried out in Image Pro^®-Plus software allowed for characterization of the surface conditions of the assessed samples in terms of their scattering properties. The obtained experimental results confirmed the usefulness of the ARS method used in the presented studies as well as the possibility of its practical use (after appropriate modifications) on a wider scale, especially in industrial applications.