Indentation recovery in GdPO4 and observation of deformation twinning

oleh: Taylor M. Wilkinson, Matthew A. Musselman, Lynn A. Boatner, David R. Diercks, Corinne E. Packard

Format: Article
Diterbitkan: AIP Publishing LLC 2016-09-01

Deskripsi

A series of nanoindentation tests on both single and polycrystalline specimens of a monazite rare-earth orthophosphate, GdPO4, revealed frequent observation of anomalous unloading behavior with a large degree of recovery, where previously this behavior had only been observed in xenotime-structure rare-earth orthophosphates. An indentation site in the polycrystalline sample was examined using TEM to identify the deformation mechanism responsible for recovery. The presence of a twin along the (100) orientation, along with a series of stacking faults contained within the deformation site, provide evidence that the mechanism of recovery in GdPO4 is the collapse of deformation twins during unloading.